By Bertil Aronsson, Torsten Lundström, Ingvar Engström (auth.), Fred W. Vahldiek, Stanley A. Mersol (eds.)

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Additional resources for Anisotropy in Single-Crystal Refractory Compounds: Proceedings of an International Symposium on Anisotropy in Single-Crystal Refractory Compounds, held on June 13–15, 1967, in Dayton Ohio. Sponsored by the Ceramics and Branch of the air Force Materials La

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W: ~_ ~L • 't ~~.... _ : .. \4 3 w/o / B-2 0 Fig. 7. Ta distribution, single crystal MozC, C-8 (CS), edge. _V V. ...... • ;; 60 __ 7Q~ _ _ _ _ 50 _. __ . < :...... - _ _ - _ . I ,! __ 2 _____ ~. l _ _ _ _ _ _ . -/ hU <&r

The solubility of carbon in MeB 2 phases is negligible; this is consistent with the general observation that carbon does not form close contacts with nonmetal atoms in the phases under discussion. One expects ~ fortiori that carbon does not dissolve to a significant extent in the boron-rich phases described in the previous section. Boron, on the other hand, can replace a fraction of the carbon atoms in the refractory MeC carbides, although the octahedral environment of the non-metal atoms in MeC is not exhibited by borides (the earlier reported NaCl-type phases TiB, ZrB and HfB do not exist).

A chemical analysis of the excited area is afforded by analysis of the characteristic x-ray lines by means of a single crystal x-ray spectrometer. The original development of the electron microprobe allowed the analysis of all elements from Na to U in the periodic table. In the last year or two this analytical range has been extended to include the light elements B, C, N, 0, F and Ne. Analysis of the light elements is an extremely important additional capability of the microprobe and it would be well to review briefly the analytical components required.

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